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Preparation of the test solution
Place an aliquot portion containing 25 to 100 mg Mo in a 250 ml beaker. Make up the volume to 50 ml with water.
Adjust this solution to pH 5 by adding the sulfuric acid solution (4.1) drop by drop. Add 15 ml of EDTA solution (4.4) and then 5 ml of buffer solution (4.5). Make up to about 80 ml with water.
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