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The Fertilisers (Sampling and Analysis) Regulations 1996
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Preparation of the solution for analysis
7.1 Weigh, to the nearest 0.001 g, 2.5 g of the prepared sample into a small glass mortar. Grind the sample three times with water, pouring off the water after each grinding into the 500 ml graduated flask (5.2). Transfer the sample quantitatively into the flask, washing the mortar, pestle and funnel with water. Make up with water to approximately 400 ml. Add 15 ml acetic acid (4.1). Shake on the rotary shaker (5.3) for two hours.
Make up to 500 ml with water, mix and filter. Discard the first portion of the filtrate.
Proceed immediately to 7.2.
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