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Commission Directive of 25 July 1980 relating to the Community method of analysis for determining the erucic acid content in oils and fats intended to be used as such for human consumption and foodstuffs containing added oils or fats (80/891/EEC) (repealed)

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  6. SignaturePrevious MatchNext Match

    1. ANNEXPrevious MatchNext Match

      THE DETERMINATION OF THE ERUCIC ACID CONTENT IN OILS AND FATS INTENDED TO BE USED AS SUCH FOR HUMAN CONSUMPTION AND IN THE FAT OR OIL COMPONENT OF FOODSTUFFS TO WHICH OILS OR FATS HAVE BEEN ADDEDPrevious MatchNext Match

      1. I. INTRODUCTION Previous MatchNext Match

        1. 1. SAMPLE PREPARATION Previous MatchNext Match

          1. 1.1. General Previous MatchNext Match

          2. 1.2. Preparation of the sample for analysis in the laboratory Previous MatchNext Match

          3. 1.3. Containers Previous MatchNext Match

        2. 2. REAGENTS Previous MatchNext Match

          1. 2.1. Water Previous MatchNext Match

            1. 2.1.1. . . . . . . . . . ....Previous MatchNext Match

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          2. 2.2. Chemicals Previous MatchNext Match

        3. 3. APPARATUS Previous MatchNext Match

          1. 3.1. List of apparatus Previous MatchNext Match

          2. 3.2. Analytical balance Previous MatchNext Match

        4. 4. EXPRESSION OF THE RESULTS Previous MatchNext Match

          1. 4.1. Results Previous MatchNext Match

          2. 4.2. Calculation of the percentage Previous MatchNext Match

          3. 4.3. Number of significant figures Previous MatchNext Match

      2. II. DETERMINATION OF ERUCIC ACID Previous MatchNext Match

        1. 1. SCOPE AND FIELD OF APPLICATION Previous MatchNext Match

        2. 2. DEFINITION Previous MatchNext Match

        3. 3. PRINCIPLE Previous MatchNext Match

        4. 4. REAGENTS Previous MatchNext Match

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        5. 5. APPARATUS Previous MatchNext Match

          1. 5.1. Apparatus for thin-layer chromatography to include, in particular: Previous MatchNext Match

          2. 5.2. . . . . . . . . . ....Previous MatchNext Match

        6. 6. PROCEDURE Previous MatchNext Match

          1. 6.1. Preparation of fatty-acid methyl esters Previous MatchNext Match

          2. 6.2. Thin-layer chromatography Previous MatchNext Match

            1. 6.2.1. Preparation of plates Previous MatchNext Match

            2. 6.2.2. Application of methyl esters Previous MatchNext Match

            3. 6.2.3. Development of the plates Previous MatchNext Match

            4. 6.2.4. Separation of the methyl ester fractions Previous MatchNext Match

          3. 6.3. Gas-liquid chromatography Previous MatchNext Match

            1. 6.3.1. . . . . . . . . . ....Previous MatchNext Match

            2. 6.3.2. Obtain from the electronic integrator the following peak areas: Previous MatchNext Match

        7. 7. EXPRESSION OF RESULTS Previous MatchNext Match

          1. 7.1. Method of calculation and formula Previous MatchNext Match

            1. 7.1.1. The erucic acid content of the sample, expressed in terms...Previous MatchNext Match

            2. 7.1.2. If peak areas are obtained in percentages the values for...Previous MatchNext Match

            3. 7.1.3. The method of calculation (7.1.1) assumes that the level of...Previous MatchNext Match

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