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4.4 Shake the sieve for 5 minutes, frequently tapping the side. Disintegrate soft lumps such as can be caused to crumble by the application of the fibres of a soft brush, taking care that the hard part of the brush does not make contact with the sieve and that the brush is not used to brush particles through the sieve. Brush out the powder in the lower receiver and weigh. Replace the receiver and repeat the shaking and tapping procedure for 2 minutes. Add the powder in the receiver to the first portion and weigh. Repeat the process until not more than 0.04 g passes through the sieve during 2 minutes.
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