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The Feeding Stuffs (Sampling and Analysis) Regulations 1999

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apparatus

4.—4.1 250 ml conical flasks with ground glass or PTFE stoppers.

4.2 Stoppered centrifuge tubes.

4.3 Gas chromatograph with flame ionisation detector.

4.4 Column:

  • either (i) 1.5 m glass column (4 mm internal diameter) packed with 5% QV17 on Gas Chrom Q, 80–100 mesh,

  • or (ii) 1.5 m glass column (4 mm internal diameter) packed with 5% Carbowax 20M-TPA on Diatomite C-AAW, 80–100 mesh.

4.5 Water bath: hotplate stirrer on which is placed a 2,000 ml beaker (or suitable vessel) containing water maintained at 40–50°C.

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