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Second Commission Directive of 18 November 1971 establishing Community methods of analysis for the official control of feedingstuffs (71/393/EEC) (repealed)

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  1. Introductory Text

  2. Article 1.. . . . . . . . . ....

  3. Article 2.. . . . . . . . . ....

  4. Article 3.. . . . . . . . . ....

    1. ANNEX

      1. I. DETERMINATION OF MOISTURE

        1. 1. Purpose and Scope

        2. 2. Principle

        3. 3. Apparatus

          1. 3.1. . . . . . . . . . ....

          2. 3.2. . . . . . . . . . ....

          3. 3.3. . . . . . . . . . ....

          4. 3.4. . . . . . . . . . ....

          5. 3.5. . . . . . . . . . ....

          6. 3.6. . . . . . . . . . ....

        4. 4. Procedure

          1. 4.1. Preparation

            1. 4.1.1. Feedingstuffs other than those coming under 4.1.2 and 4.1.3

            2. 4.1.2. Cereals and groats

            3. 4.1.3. Feedingstuffs in liquid or paste form, feedingstuffs predominantly composed of...

          2. 4.2. Drying

            1. 4.2.1. Feedingstuffs other than those coming under 4.2.2 and 4.2.3

            2. 4.2.2. Cereals, flour, groats and meal

            3. 4.2.3. Compound feedingstuffs containing more than 4% of sucrose or lactose:...

          3. 4.3. Preliminary drying

            1. 4.3.1. Feedingstuffs other than those coming under 4.3.2

            2. 4.3.2. Cereals

        5. 5. Calculation of results

          1. 5.1. Drying without preliminary drying

          2. 5.2. Drying with preliminary drying

          3. 5.3. Repeatibility

        6. 6. Observation

      2. II. DETERMINATION OF VOLATILE NITROGENOUS BASES

        1. A. MICRODIFFUSION

          1. 1. Purpose and Scope

          2. 2. Principle

          3. 3. Reagents

            1. 3.1. . . . . . . . . . ....

            2. 3.2. . . . . . . . . . ....

            3. 3.3. . . . . . . . . . ....

            4. 3.4. . . . . . . . . . ....

            5. 3.5. . . . . . . . . . ....

          4. 4. Apparatus

            1. 4.1. . . . . . . . . . ....

            2. 4.2. . . . . . . . . . ....

            3. 4.3. . . . . . . . . . ....

          5. 5. Procedure

          6. 6. Calculation of results

            1. Repeatibility

          7. 7. Observation

          8. CONWAY CELL Scale 1/1

        2. B. BY DISTILLATION

          1. 1. Purpose and Scope

          2. 2. Principle

          3. 3. Reagents

            1. 3.1. . . . . . . . . . ....

            2. 3.2. . . . . . . . . . ....

            3. 3.3. . . . . . . . . . ....

            4. 3.4. . . . . . . . . . ....

            5. 3.5. . . . . . . . . . ....

            6. 3.6. . . . . . . . . . ....

          4. 4. Apparatus

            1. 4.1. . . . . . . . . . ....

            2. 4.2. . . . . . . . . . ....

          5. 5. Procedure

          6. 6. Calculation of results

            1. Repeatibility

      3. III. DETERMINATION OF TOTAL PHOSPHORUS

        1. 1. Purpose and Scope

        2. 2. Principle

        3. 3. Reagents

          1. 3.1. . . . . . . . . . ....

          2. 3.2. . . . . . . . . . ....

          3. 3.3. . . . . . . . . . ....

          4. 3.4. . . . . . . . . . ....

          5. 3.5. . . . . . . . . . ....

          6. 3.6. . . . . . . . . . ....

            1. 3.6.1. . . . . . . . . . ....

            2. 3.6.2. . . . . . . . . . ....

          7. 3.7. . . . . . . . . . ....

        4. 4. Apparatus

          1. 4.1. . . . . . . . . . ....

          2. 4.2. . . . . . . . . . ....

          3. 4.3. . . . . . . . . . ....

          4. 4.4. . . . . . . . . . ....

          5. 4.5. . . . . . . . . . ....

          6. 4.6. . . . . . . . . . ....

        5. 5. Procedure

          1. 5.1. Preparation of the solution

            1. 5.1.1. Usual procedure

            2. 5.1.2. Samples containing organic substances and free from calcium and magnesium...

          2. 5.2. Development of coloration and measurement of optical density

          3. 5.3. Calibration curve

        6. 6. Calculation of results

          1. Repeatibility

      4. IV. DETERMINATION OF CRUDE OILS AND FATS

        1. 1. Purpose and scope

          1. 1.1. Procedure A — Directly extractable crude oils and fats

          2. 1.2. Procedure B — Total crude oils and fats

          3. 1.3. Interpretation of results

        2. 2. Principle

          1. 2.1. Procedure A

          2. 2.2. Procedure B

        3. 3. Reagents

          1. 3.1. . . . . . . . . . ....

          2. 3.2. . . . . . . . . . ....

          3. 3.3. . . . . . . . . . ....

          4. 3.4. . . . . . . . . . ....

        4. 4. Apparatus

          1. 4.1. . . . . . . . . . ....

          2. 4.2. . . . . . . . . . ....

          3. 4.3. . . . . . . . . . ....

        5. 5. Procedure

          1. 5.1. Procedure A (see point 8.1)

          2. 5.2. Procedure B

        6. 6. Expression of result

        7. 7. Repeatability

        8. 8. Observations

          1. 8.1. . . . . . . . . . ....

          2. 8.2. . . . . . . . . . ....

          3. 8.3. . . . . . . . . . ....

          4. 8.4. . . . . . . . . . ....

          5. 8.5. . . . . . . . . . ....

          6. 8.6. . . . . . . . . . ....

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