SCHEDULE 2METHODS OF ANALYSIS

PART I

25d.DETERMINATION OF TRACE ELEMENTS IN FERTILISER EXTRACTS BY ATOMIC ABSORPTION SPECTROMETRY (GENERAL PROCEDURE)

EXPRESSION OF RESULTS8

The percentage of trace element (E) in the fertiliser is equal to:

E(%)=[(xs-xb)×V×D]/(M×104).

If method (25c) has been used:

E(%)=[(xs-xb)×V×2D]/(M×104),

where:

  • E is the amount of the trace element determined, expressed as a percentage of the fertiliser;

  • xs is the concentration of the test solution (6.2), in μg/ml;

  • xb is the concentration of the blank solution (7.1), in μg/ml;

  • V is the volume of the extract obtained by Method 25a or 25b, in ml;

  • D is the factor corresponding to the dilution carried out in (6.2);

  • M is the mass of the test sample taken in accordance with Method 25a or 25b in grams.

Calculation of dilution factor D:

If (a1), (a2), (a3), . . ., (ai) and (a) are the aliquot portions and (v1), (v2), (v3), . . ., (vi) and (100) are the volumes in ml corresponding to their respective dilutions, the dilution factor D will be equal to:

D=(v1/a1)×(v2/a2)×(v3/a3)×...×(vi/ai)×(100/a).