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Commission Regulation (EU) 2019/1102Show full title

Commission Regulation (EU) 2019/1102 of 27 June 2019 amending Regulation (EC) No 2003/2003 of the European Parliament and of the Council relating to fertilisers for the purposes of adapting Annexes I and IV (Text with EEA relevance)

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ANNEX IIU.K.

In Annex IV to Regulation (EC) No 2003/2003, Section B is amended as follows:

(1)

Method 1 is replaced by the following:

Methods 1Sample preparation and sampling

Method 1.1 Sampling for analysis

EN 1482-1, Fertilizers and liming materials — Sampling and sample preparation — Part 1: Sampling

Method 1.2Preparation of sample for analysis

EN 1482-2, Fertilizers and liming materials — Sampling and sample preparation — Part 2: Sample preparation

Method 1.3 Sampling of static heaps for analysis

EN 1482-3, Fertilizers and liming materials — Sampling and sample preparation — Part 3: Sampling of static heaps

(2)

Methods 9 are replaced by the following:

Methods 9Micro-nutrients at a concentration of less than or equal to 10 %

Method 9.1 Extraction of total micro-nutrients in fertilisers using aqua regia

EN 16964: Fertilizers — Extraction of total micro-nutrients in fertilizers using aqua regia

This method of analysis has been ring-tested.

Method 9.2 Extraction of water soluble micro-nutrients in fertilisers and removal of organic compounds from fertilizer extracts

EN 16962: Fertilizers — Extraction of water soluble micro-nutrients in fertilizers and removal of organic compounds from fertilizer extracts

This method of analysis has been ring-tested.

Method 9.3 Determination of cobalt, copper, iron, manganese and zinc using flame atomic absorption spectrometry (FAAS)

EN 16965: Fertilizers — Determination of cobalt, copper, iron, manganese and zinc using flame atomic absorption spectrometry (FAAS)

This method of analysis has been ring-tested

Method 9.4 Determination of boron, cobalt, copper, iron, manganese, molybdenum and zinc using ICP-AES

EN 16963: Fertilizers — Determination of boron, cobalt, copper, iron, manganese, molybdenum and zinc using ICP-AES

This method of analysis has been ring-tested.

Method 9.5 Determination of boron using spectrometry with azomethine-H

EN 17041: Fertilizers — Determination of boron in concentrations ≤ 10 % using spectrometry with azomethine-H

This method of analysis has been ring-tested.

Method 9.6 Determination of molybdenum using spectrometry of a complex with ammonium thiocyanate

EN 17043: Fertilizers — Determination of molybdenum in concentrations in concentrations ≤ 10 % using spectrometry of a complex with ammonium thiocyanate

This method of analysis has been ring-tested.

(3)

Methods 10 are replaced by the following:

Methods 10 Micro-nutrients at a concentration greater than 10 %

Method 10.1 Extraction of total micro-nutrients in fertilisers using aqua regia

EN 16964: Fertilizers — Extraction of total micro-nutrients in fertilizers using aqua regia

This method of analysis has been ring-tested.

Method 10.2 Extraction of water soluble micro-nutrients in fertilisers and removal of organic compounds from fertilizer extracts

EN 16962: Fertilizers — Extraction of water soluble micro-nutrients in fertilizers and removal of organic compounds from fertilizer extracts

This method of analysis has been ring-tested.

Method 10.3 Determination of cobalt, copper, iron, manganese and zinc using flame atomic absorption spectrometry (FAAS)

EN 16965: Fertilizers — Determination of cobalt, copper, iron, manganese and zinc using flame atomic absorption spectrometry (FAAS)

This method of analysis has been ring-tested.

Method 10.4 Determination of boron, cobalt, copper, iron, manganese, molybdenum and zinc using ICP-AES

EN 16963: Fertilizers — Determination of boron, cobalt, copper, iron, manganese, molybdenum and zinc using ICP-AES

This method of analysis has been ring-tested.

Method 10.5 Determination of boron using acidimetric titration

EN 17042: Fertilizers — Determination of boron in concentrations > 10 % using acidimetric titration

This method of analysis has not been ring-tested.

Method 10.6 Determination of molybdenum using gravimetric method with 8-hydroxyquinoline

CEN/TS 17060: Fertilizers — Determination of molybdenum in concentration > 10 % using gravimetric method with 8-hydroxyquinoline

This method of analysis has not been ring-tested.

(4)

In Methods 12, Method 12.8 is added:

Method 12.8 Determination of DMPSA

EN 17090: Fertilizers — Determination of nitrification inhibitor DMPSA in fertilizers — Method using high-performance liquid chromatography (HPLC)

This method of analysis has been ring-tested.

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