3.APPARATUS AND REAGENTS (other than those specified in the general instructions)U.K.
3.1.ApparatusU.K.
Glass-stoppered conical flask of at least 200 ml capacity.
3.2.ReagentsU.K.
(a)Sulphuric acid (75 ± 2 % m/m)U.K.
Prepare by adding carefully, while cooling, 700 ml sulphuric acid (relative density at 20 °C: 1,84) to 350 ml distilled water.
After cooling to room temperature, dilute the solution to 1 litre with water.