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SCHEDULE 2METHODS OF ANALYSIS

PART II

2.DETERMINATION OF MOISTURE

SCOPE AND FIELD OF APLICATION

1.  This method is applicable to all fertilisers where a correction for moisture is necessary.

PRINCIPLE

2.  The sample is dried to constant weight in an oven at 100°C. The loss in weight corresponds to the moisture content of the sample.

APPARATUS

3.—3.1 Suitable containers with lids ensuring air tight closure; the dimensions should allow the sample to be spread at about 0.3 g per cm2.

3.2 Electrically heated oven, suitably ventilated and capable of being maintained at 100±2°C.

PREPARATION OF SAMPLE

4.  See Method 1.

PROCEDURE

5.  Weigh to the nearest 0.001 g, 5 g of the prepared sample and transfer to a previously weighed container (3.1). Place the uncovered container and the lid in the oven (3.2) for 2 to 3 hours. Replace the lid on the container, remove from the oven and allow to cool in a desiccator and weigh. Reheat for another hour, cool and reweigh. If the difference in weight exceeds 0.01g continue the heating and cooling procedure until a weight constant within 0.01 g is attained.

EXPRESSION OF RESULT

6.  Calculate the total loss of weights and express it as a percentage of the original weight.